[Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2

Base Information

Chemical Name:[Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2
CAS No.:97732-43-9
Molecular Formula:C₂₂H₅₂Mo₂O₄P₄
Molecular Weight:696.428
Hs Code.:

[Mo(H)(P(CH<sub>3</sub>)3)2(CH<sub>2</sub>CH<sub>2</sub>)(CH<sub>2</sub>CHC(O)O)]2

Synonyms:[Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2

Suppliers and Price of [Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2

Chemical Property:

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Technology Process of [Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2

There total 1 articles about [Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 82044-79-9
trans-{Mo(ethylene)2(P(CH₃)3)4}

: 97732-43-9
[Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2

: 594-09-2
trimethylphosphane

Guidance literature:: With CO₂; In diethyl ether; under N2, CO2 bubbling through soln. of ethene complex, -20°C, 20 min; filtering off ppt. at low temp., drying in vac., washing with petroleum ether (2nd crop from mother liquor), recrystn. from diethyl ether; elem. anal.;

Reference yield:

: 97732-43-9
[Mo(H)(P(CH₃)3)2(CH₂CH₂)(CH₂CHC(O)O)]2

: 74-85-1
ethene

: 594-09-2
trimethylphosphane

: 82044-79-9
trans-{Mo(ethylene)2(P(CH₃)3)4}

: 13270-28-5
Lithium acrylate

Guidance literature:: With n-C₄H₉Li; In benzene; byproducts: n-C4H10; under atmosphere of ethylene, successive addn. of PMe3 and n-C4H9Li (0.9 M in hexane) to soln. of acrylate complex, room temp., stirring, 40-50 min, evapn. of solvent in vac., extg. with petroleum ether (residue: Li acrylate); products identified by IR and 1H NMR (Li acrylate) and 31P NMR, resp.;