{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*BF₄^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}BF₄

Base Information

• Chemical Name: {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*BF₄^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}BF₄
• CAS No.: 110391-73-6
• Molecular Formula: BF₄*C₄₈H₅₅ClP₄RhS₂
• Molecular Weight: 1045.15

Synonyms:{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*BF₄^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}BF₄

Chemical Property of {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*BF₄^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}BF₄

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Technology Process of {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*BF₄^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}BF₄

There total 2 articles about {(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}⁽¹⁺⁾*BF₄^(1-)={(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CHP(C₂H₅)3)}BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

silver tetrafluoroborate (14104-20-2) + {(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)} (100044-10-8) → {(CH3C(CH2P(C6H5)2)3)RhCl(S2CHP(C2H5)3)}(1+)*BF4(1-)={(CH3C(CH2P(C6H5)2)3)RhCl(S2CHP(C2H5)3)}BF4 (110391-73-6)

Guidance literature:

With ethanol; In tetrahydrofuran; byproducts: Ag; a 2-fold excess of AgBF4 in THF was added to a stirred soln. of ((triphos)RhCl(S2CPEt3)) in THF; filtration; addn. of ethanol to the filtrate; mechanism discussed;; dried in a stream of N2;;

Reference yield: 70.0%

{(CH3C(CH2P(C6H5)2)3)RhCl(S2CP(C2H5)3)} (100044-10-8) + nitrosonium tetrafluoroborate → {(CH3C(CH2P(C6H5)2)3)RhCl(S2CHP(C2H5)3)}(1+)*BF4(1-)={(CH3C(CH2P(C6H5)2)3)RhCl(S2CHP(C2H5)3)}BF4 (110391-73-6)

Guidance literature:

With ethanol; In dichloromethane; stirring a soln. of ((triphos)RhCl(S2CPEt3)) and NOBF4 in CH2Cl2 for 1 h; filtration; addn. of ethanol to the filtrate; mechanism discussed;; slow evapn. of the solvents; filtration; washed with ethanol and petroleum ether; dried in a stream of N2; elem. anal.;;

upstream raw materials:

{(CH₃C(CH₂P(C₆H₅)2)3)RhCl(S₂CP(C₂H₅)3)}

silver tetrafluoroborate

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