6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide

Base Information

Chemical Name:6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide
CAS No.:1374004-87-1
Molecular Formula:C₄₀H₃₂N₂O₅
Molecular Weight:620.704
Hs Code.:

Synonyms:6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide

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Chemical Property of 6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide

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Technology Process of 6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide

There total 9 articles about 6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1374004-88-2
N-benzyl-2-(5-benzyloxy-4-[2-(4-benzyloxy-3-methoxy-phenyl)-acetyl]-1H-indol-3-yl)-2-oxo-acetamide

: 1374004-87-1
6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide

Guidance literature:: With potassium carbonate; In tetrahydrofuran; for 2h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.03.026

Reference yield:

: C₃₃H₂₆ClNO₆

: 1374004-87-1
6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

2: potassium carbonate / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

With potassium carbonate; In tetrahydrofuran;
DOI:10.1016/j.tet.2012.03.026

Reference yield:

: 1374004-96-2
1-(5-benzyloxy-1H-indol-4-yl)-2-(4-benzyloxy-3-methoxy-phenyl)-ethanone

: 1374004-87-1
6-benzyloxy-4-(4-benzyloxy-3-methoxy-phenyl)-5-oxo-1,5-dihydro-benzo[cd]indole-3-carboxylic acid benzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

2: tetrahydrofuran / 0.17 h / 20 °C / Inert atmosphere

3: potassium carbonate / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

With potassium carbonate; In tetrahydrofuran;
DOI:10.1016/j.tet.2012.03.026