methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate

Base Information

Chemical Name:methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate
CAS No.:1255910-56-5
Molecular Formula:C₃₃H₅₂O₄Si₂
Molecular Weight:568.944
Hs Code.:

Synonyms:methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate

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Technology Process of methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate

There total 1 articles about methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 994-30-9
triethylsilyl chloride

: 1255910-69-0
methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-6-hydroxy-7-methylnon-2-enoate

: 1255910-56-5
methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate

Guidance literature:: With pyridine; dmap; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol102177j

Reference yield: 80.0%

: 1255910-56-5
methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate

: 75-16-1
methylmagnesium bromide

: 1255910-59-8
methyl (3S,7R)-9-(tert-butyldiphenylsilyloxy)-3,7-dimethyl-6-(triethylsilyloxy)nonanoate

Guidance literature:: methylmagnesium bromide; With copper(l) iodide; 1,1′-binaphthalene-2,2′-diylbis[bis(4-methylphenyl)phosphine]; In diethyl ether; tert-butyl methyl ether; at -20 ℃; for 0.25h; Inert atmosphere;

methyl (7R,E)-9-(tert-butyldiphenylsilyloxy)-7-methyl-6-(triethylsiloxy)non-2-enoate; In diethyl ether; tert-butyl methyl ether; at -20 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol102177j