tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

Base Information

Chemical Name:tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate
CAS No.:1444764-55-9
Molecular Formula:C₃₈H₅₀Br₂N₆O₈
Molecular Weight:878.658
Hs Code.:

Synonyms:tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

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Chemical Property of tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

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Technology Process of tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

There total 2 articles about tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 13472-00-9
p-Aminophenethylamine

: 1444764-51-5
diethyl 2,2'-(((4-bromo-6-(bromomethyl)pyridin-2-yl)methyl)azanediyl)diacetate

: 1444764-55-9
tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

Guidance literature:: With potassium carbonate; In acetonitrile; at 50 - 55 ℃; for 4h;

Reference yield:

: 6290-05-7
Diethyl iminodiacetate

: 106967-42-4
4-bromo-2,6-bis(bromomethyl)pyridine

: 1444764-55-9
tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

Guidance literature:: Multi-step reaction with 2 steps

1: acetonitrile / 2.5 h / 60 - 65 °C

2: potassium carbonate / acetonitrile / 4 h / 50 - 55 °C

With potassium carbonate; In acetonitrile;

Reference yield: 22.0%

: 1425510-29-7
diethyl 2,2'-{[4-(ethynyl)-1,3-phenylene]bis(oxy)}diacetate

: 1444764-55-9
tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-bromopyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

: 1444764-59-3
tetraethyl 2,2',2,2'-(((6,6'-(((4-aminophenethyl)azanediyl)bis(methylene))bis(4-((2,4-bis(2-ethoxy-2-oxoethoxy)phenyl)ethynyl)pyridine-6,2-diyl))bis(methylene))bis(azanetriyl))tetraacetate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In tetrahydrofuran; at 55 ℃; Inert atmosphere;