Technology Process of C45H55N3
There total 3 articles about C45H55N3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis(diphenylphosphino)biphenyl;
In
toluene;
at 90 ℃;
for 48h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / palladium diacetate; CyJohnPhos / 1,4-dioxane / 2.5 h / 80 °C
2: barium dihydroxide / 1,4-dioxane; water / 20 h / 20 - 100 °C
3: sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis(diphenylphosphino)biphenyl / toluene / 48 h / 90 °C
With
barium dihydroxide; triethylamine; sodium t-butanolate;
palladium diacetate; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis(diphenylphosphino)biphenyl; CyJohnPhos;
In
1,4-dioxane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: barium dihydroxide / 1,4-dioxane; water / 20 h / 20 - 100 °C
2: sodium t-butanolate / tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis(diphenylphosphino)biphenyl / toluene / 48 h / 90 °C
With
barium dihydroxide; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis(diphenylphosphino)biphenyl;
In
1,4-dioxane; water; toluene;