2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

Base Information

Chemical Name:2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene
CAS No.:392335-73-8
Molecular Formula:C₃₆H₆₈GeOSi₆
Molecular Weight:758.038
Hs Code.:

Synonyms:2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

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Chemical Property of 2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

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Technology Process of 2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

There total 6 articles about 2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 392335-69-2
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-2-germanaphthalene

: 7732-18-5
water

: 392335-73-8
2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

Guidance literature:: In not given;
DOI:10.1021/om010881y

Reference yield:

: 392335-70-5
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2,3,4-tetrahydro-2-germanaphthalene

: 392335-73-8
2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

Guidance literature:: Multi-step reaction with 4 steps

1: NBS; LiAlH₄; t-BuLi / tetrahydrofuran

2: BPO / benzene

3: LDA / tetrahydrofuran

4: not given

With NBS; LiAlH₄; t-BuLi; BPO; LDA; In tetrahydrofuran; benzene;
DOI:10.1021/om010881y

Reference yield:

: 392335-71-6
2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

: 392335-73-8
2-hydroxy-2-[2,4,6-tris(bis(trimethylsilyl)methyl)phenyl]-1,2-dihydro-2-germanaphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: BPO / benzene

2: LDA / tetrahydrofuran

3: not given

With BPO; LDA; In tetrahydrofuran; benzene;
DOI:10.1021/om010881y