5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one

Base Information

• Chemical Name: 5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one
• CAS No.: 1380392-05-1
• Molecular Formula: C₂₅H₂₆ClN₃O
• Molecular Weight: 419.954

Synonyms:5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one

Chemical Property of 5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one

Chemical Property:

• Boiling Point: 603.8±55.0 °C(Predicted)
• Density: 1.26±0.1 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

JMS-17-2 >98% ^*data from reagent suppliers

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Technology Process of 5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one

There total 2 articles about 5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

4-(4-chlorophenyl)piperidine (26905-02-2) + 5-(3-chloropropyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one (1380392-06-2) → 5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one (1380392-05-1)

Guidance literature:

With potassium carbonate; In acetonitrile; at 140 ℃; for 1h; Microwave irradiation; Sealed tube;

Reference yield:

pyrrolo<1,2-a>quinoxalin-4(5H)-one (6025-68-9) → 5-(3-(4-(4-chlorophenyl)piperidin-1-yl)propyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one (1380392-05-1)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 2 h / 20 °C / Inert atmosphere

1.2: 12 h / 80 °C / Inert atmosphere

2.1: potassium carbonate / acetonitrile / 1 h / 140 °C / Microwave irradiation; Sealed tube

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetonitrile; mineral oil;

upstream raw materials:

4-(4-chlorophenyl)piperidine

5-(3-chloropropyl)pyrrolo[1,2-a]quinoxalin-4(5H)-one

pyrrolo<1,2-a>quinoxalin-4(5H)-one

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