C₃₅H₅₀N₂O₅

Base Information

Chemical Name:C₃₅H₅₀N₂O₅
CAS No.:1579830-48-0
Molecular Formula:C₃₅H₅₀N₂O₅
Molecular Weight:578.792
Hs Code.:

C<sub>35</sub>H<sub>50</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₃₅H₅₀N₂O₅

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Chemical Property of C₃₅H₅₀N₂O₅

Chemical Property:

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Technology Process of C₃₅H₅₀N₂O₅

There total 10 articles about C₃₅H₅₀N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1579830-33-3
C₂₇H₄₁ClO₂

: 69397-93-9
N-methyl-5-methoxy-2-nitroaniline

: 1579830-48-0
C₃₅H₅₀N₂O₅

Guidance literature:: With pyridine; In toluene; at 120 ℃;
DOI:10.1002/anie.201307465

Reference yield:

: 14773-00-3
methyl (5β,7α)-12-hydroxy-3-oxo-cholan-24-oate

: 1579830-48-0
C₃₅H₅₀N₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0.25 h / 20 °C

1.2: 0 °C

2.1: 2-iodoxybenzoic acid; trifluoroacetic acid / dimethyl sulfoxide / 60 °C / Darkness

3.1: lithium; ammonia / tert-butyl alcohol; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 0.25 h / 20 °C

4.2: 20 °C

5.1: Burgess Reagent / toluene / Reflux

6.1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

7.1: methanol / 0.25 h / Inert atmosphere

7.2: 3.02 h / 50 °C

8.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.33 h / Inert atmosphere

9.1: pyridine / toluene / 120 °C

With pyridine; oxalyl dichloride; Burgess Reagent; 2-iodoxybenzoic acid; ammonia; lithium; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 5.1: |Burgess Alcohol Dehydration;
DOI:10.1002/anie.201307465

Reference yield:

: 1228360-87-9
methyl 3-oxo-7α-benzyloxymethyl-5β-cholan-24-oate

: 1579830-48-0
C₃₅H₅₀N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2-iodoxybenzoic acid; trifluoroacetic acid / dimethyl sulfoxide / 60 °C / Darkness

2.1: lithium; ammonia / tert-butyl alcohol; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; lithium chloride / acetonitrile / 0.25 h / 20 °C

3.2: 20 °C

4.1: Burgess Reagent / toluene / Reflux

5.1: lithium hydroxide / methanol; tetrahydrofuran; water / 20 °C

6.1: methanol / 0.25 h / Inert atmosphere

6.2: 3.02 h / 50 °C

7.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 0.33 h / Inert atmosphere

8.1: pyridine / toluene / 120 °C

With pyridine; oxalyl dichloride; Burgess Reagent; 2-iodoxybenzoic acid; ammonia; lithium; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; lithium chloride; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 4.1: |Burgess Alcohol Dehydration;
DOI:10.1002/anie.201307465