ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate

Base Information

Chemical Name:ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate
CAS No.:1391001-14-1
Molecular Formula:C₁₇H₂₁Cl₂NO₄
Molecular Weight:374.264
Hs Code.:

Synonyms:ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate

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Chemical Property of ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate

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Technology Process of ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate

There total 3 articles about ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391001-13-0
methyl 3-amino-4-(2,6-dichlorophenyl)butanoate

: 141-97-9
ethyl acetoacetate

: 1391001-14-1
ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate

Guidance literature:: With magnesium sulfate; acetic acid; In toluene; at 110 ℃; for 3h;

Reference yield:

: 221121-45-5
ethyl 4-(2,6-dichlorophenyl)-3-oxobutanoate

: 1391001-14-1
ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: magnesium sulfate; sodium cyanoborohydride; ammonium acetate / 18 h / 70 °C

2: magnesium sulfate; acetic acid / toluene / 3 h / 110 °C

With ammonium acetate; sodium cyanoborohydride; magnesium sulfate; acetic acid; In toluene;

Reference yield:

: 6575-24-2
2-(2,6-dichlorophenyl)acetic acid

: 1391001-14-1
ethyl 3-(1-(methoxycarbonyl)-3-(2,6-dichlorophenyl)propan-2-ylamino)but-2-enoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 1 h / 20 °C

1.2: 18 h / 70 °C

2.1: magnesium sulfate; sodium cyanoborohydride; ammonium acetate / 18 h / 70 °C

3.1: magnesium sulfate; acetic acid / toluene / 3 h / 110 °C

With ammonium acetate; sodium cyanoborohydride; magnesium sulfate; acetic acid; 1,1'-carbonyldiimidazole; In tetrahydrofuran; toluene;