ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate

Base Information

Chemical Name:ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate
CAS No.:1391001-16-3
Molecular Formula:C₁₆H₁₅Cl₂NO₃
Molecular Weight:340.206
Hs Code.:

Synonyms:ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate

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Chemical Property of ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate

Chemical Property:

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Technology Process of ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate

There total 5 articles about ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1391001-15-2
ethyl 6-(2,6-dichlorobenzyl)-1,4,5,6-tetrahydro-2-methyl-4-oxopyridine-3-carboxylate

: 1391001-16-3
ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; at 20 ℃; for 18.08h;

Reference yield:

: 221121-45-5
ethyl 4-(2,6-dichlorophenyl)-3-oxobutanoate

: 1391001-16-3
ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: magnesium sulfate; sodium cyanoborohydride; ammonium acetate / 18 h / 70 °C

2: magnesium sulfate; acetic acid / toluene / 3 h / 110 °C

3: potassium tert-butylate / tetrahydrofuran / 18 h / 20 °C

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 18.08 h / 20 °C

With potassium tert-butylate; ammonium acetate; sodium cyanoborohydride; magnesium sulfate; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; toluene;

Reference yield:

: 1391001-13-0
methyl 3-amino-4-(2,6-dichlorophenyl)butanoate

: 1391001-16-3
ethyl 6-(2,6-dichlorobenzyl)-1,4-dihydro-2-methyl-4-oxopyridine-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium sulfate; acetic acid / toluene / 3 h / 110 °C

2: potassium tert-butylate / tetrahydrofuran / 18 h / 20 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 18.08 h / 20 °C

With potassium tert-butylate; magnesium sulfate; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; toluene;