N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

Base Information

Chemical Name:N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine
CAS No.:1426922-40-8
Molecular Formula:C₂₁H₁₉ClN₂O₄S₂
Molecular Weight:462.978
Hs Code.:

Synonyms:N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

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Chemical Property of N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

Chemical Property:

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Technology Process of N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

There total 3 articles about N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 941-55-9
4-toluenesulfonyl azide

: 1426922-69-1
N-[2-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

: 1426922-40-8
N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

Guidance literature:: With silver hexafluoroantimonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium acetate; In 1,2-dichloro-ethane; at 120 ℃; for 24h; regioselective reaction; Schlenk technique; Glovebox;
DOI:10.1021/ol400411v

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1426922-40-8
N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / water; acetone / 0 - 20 °C / Schlenk technique

2: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium acetate; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 120 °C / Schlenk technique; Glovebox

With silver hexafluoroantimonate; sodium azide; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium acetate; In water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/ol400411v

Reference yield:

: 609-65-4
o-chlorobenzoyl chloride

: 4381-25-3
S-methyl-S-phenylsulfoximine

: 1426922-40-8
N-[2-(4'-methylbenzenesulfonamido)-6-chlorobenzoyl]-S-methyl-S-phenylsulfoximine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

1.2: 12 h / 0 - 20 °C / Inert atmosphere; Schlenk technique

2.1: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium acetate; silver hexafluoroantimonate / 1,2-dichloro-ethane / 24 h / 120 °C / Schlenk technique; Glovebox

With silver hexafluoroantimonate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium acetate; sodium hydride; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol400411v