N-isopropyl-3-phenylpropiolamide

Base Information

Chemical Name:N-isopropyl-3-phenylpropiolamide
CAS No.:88611-45-4
Molecular Formula:C₁₂H₁₃NO
Molecular Weight:187.241
Hs Code.:

Synonyms:N-isopropyl-3-phenylpropiolamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-isopropyl-3-phenylpropiolamide

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Technology Process of N-isopropyl-3-phenylpropiolamide

There total 4 articles about N-isopropyl-3-phenylpropiolamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 536-74-3
phenylacetylene

: 693-13-0
diisopropyl-carbodiimide

: 88611-45-4
N-isopropyl-3-phenylpropiolamide

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; at -30 - 20 ℃;

diisopropyl-carbodiimide; In tetrahydrofuran; at 20 ℃; for 1h;

With ammonium chloride; In tetrahydrofuran;
DOI:10.1021/ja0560027

Reference yield: 77.0%

: 591-51-5
phenyllithium

: 162375-31-7
N-iso-propyl-Z-3-chloro-2-(phenylthio)propenamide

: 88611-45-4
N-isopropyl-3-phenylpropiolamide

Guidance literature:: phenyllithium; With copper(l) iodide; In diethyl ether; at -78 ℃; for 0.166667h; Inert atmosphere;

N-iso-propyl-Z-3-chloro-2-(phenylthio)propenamide; In diethyl ether; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1039/c0ob00805b

Reference yield: 37.0%

: 75-31-0
isopropylamine

: 637-44-5
phenylpropyolic acid

: 88611-45-4
N-isopropyl-3-phenylpropiolamide

Guidance literature:: phenylpropyolic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 0.166667h;

isopropylamine; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1021/acs.orglett.9b01132