(Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

Base Information

Chemical Name:(Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide
CAS No.:1620886-78-3
Molecular Formula:C₁₇H₂₂ClNO₂
Molecular Weight:307.82
Hs Code.:

Synonyms:(Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

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Chemical Property of (Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

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Technology Process of (Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

There total 1 articles about (Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 821-09-0
n-Pent-4-enyl alcohol

: 88611-45-4
N-isopropyl-3-phenylpropiolamide

: 1620886-78-3
(Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

Guidance literature:: With copper(II) chloride dihydrate; palladium diacetate; In acetonitrile; at 20 ℃; for 12h; stereoselective reaction;
DOI:10.1021/jo501317v

Reference yield: 93.0%

: 1620886-78-3
(Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

: (Z)-3-chloro-N-isopropyl-3-phenyl-2-[(tetrahydrofuran-2-yl)methyl]prop-2-en-1-ylamine

Guidance literature:: (Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide; With 2-fluoropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 ℃; for 0.333333h;

With 1,1,3,3-Tetramethyldisiloxane; In dichloromethane; at 0 - 20 ℃; for 3.16667h;

With tris(pentafluorophenyl)borate; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/acs.joc.6b00572

Reference yield: 81.0%

: 1620886-78-3
(Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide

: (Z)-3-chloro-3-phenyl-2-[(tetrahydrofuran-2-yl)methyl]acrylaldehyde

Guidance literature:: (Z)-3-chloro-N-isopropyl-3-phenyl-2-((tetrahydrofuran-2-yl)methyl)acrylamide; With 2-fluoropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at 0 ℃; for 0.333333h; Inert atmosphere;

With 1,1,3,3-Tetramethyldisiloxane; In dichloromethane; at 0 - 20 ℃; for 6.16667h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; at 20 ℃; Inert atmosphere;
DOI:10.1007/s11426-016-0224-5