methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate

Base Information

Chemical Name:methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate
CAS No.:1041859-45-3
Molecular Formula:C₁₇H₂₃BO₅
Molecular Weight:318.178
Hs Code.:

Synonyms:methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate

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Chemical Property of methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate

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Technology Process of methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate

There total 2 articles about methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 30913-86-1
4-(4-bromo-phenyl)-4-oxo-butyric acid methyl ester

: 73183-34-3
bis(pinacol)diborane

: 1041859-45-3
methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate

Guidance literature:: With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In dimethyl sulfoxide; at 80 ℃; for 3h;
DOI:10.1021/ja802757w

Reference yield:

: 6340-79-0
4-oxo-4-(4-bromophenyl)butanoic acid

: 1041859-45-3
methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / methanol / Reflux

2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / dimethyl sulfoxide / 1 h / 80 °C / Inert atmosphere

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; potassium acetate; In methanol; dimethyl sulfoxide;

Reference yield:

: 4548-45-2
2-chloro-5-nitropyridine

: 1041859-45-3
methyl 4-oxo-4-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolane-2-yl)phenyl]butyrate

: 1357165-86-6
methyl 4-[4-(5-nitropyridin-2-yl)phenyl]-4-oxobutyrate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,2-dimethoxyethane; at 80 ℃; for 4h; Inert atmosphere;