C₂₁H₃₆O₄Si₂

Base Information

• Chemical Name: C₂₁H₃₆O₄Si₂
• CAS No.: 82112-32-1
• Molecular Formula: C₂₁H₃₆O₄Si₂
• Molecular Weight: 408.685
• Mol file: 82112-32-1.mol

Synonyms:C₂₁H₃₆O₄Si₂

Chemical Property of C₂₁H₃₆O₄Si₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₁H₃₆O₄Si₂

There total 2 articles about C₂₁H₃₆O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-hydroxyphenylpiruvic acid (156-39-8) + N-methyl-N-tert-butyldimethylsilyl-1,1,1-trifluoroacetamide (77377-52-7) → C21H36O4Si2 (82112-32-1)

Guidance literature:

With tert-butyldimethylsilyl chloride; In acetonitrile; for 0.0833333h; Ambient temperature; other silylating agent;

DOI:10.1021/jo00138a032

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → C21H36O4Si2 (82112-32-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) sodium hydride / 1.) benzene, acetonitrile, 4 deg C, 4 h, 2.) 2 h

2: 100 percent / 1percent tert-butyldimethylsilyl chloride (TBDMSCl) / acetonitrile / 0.08 h / Ambient temperature; other silylating agent

With sodium hydride; tert-butyldimethylsilyl chloride; In acetonitrile;

DOI:10.1021/jo00138a032

upstream raw materials:

4-hydroxyphenylpiruvic acid

N-methyl-N-tert-butyldimethylsilyl-1,1,1-trifluoroacetamide

tert-butyldimethylsilyl chloride