C₂₅H₃₃N₅O₃

Base Information

Chemical Name:C₂₅H₃₃N₅O₃
CAS No.:1246520-22-8
Molecular Formula:C₂₅H₃₃N₅O₃
Molecular Weight:451.569
Hs Code.:

C<sub>25</sub>H<sub>33</sub>N<sub>5</sub>O<sub>3</sub>

Synonyms:C₂₅H₃₃N₅O₃

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Chemical Property of C₂₅H₃₃N₅O₃

Chemical Property:

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Technology Process of C₂₅H₃₃N₅O₃

There total 12 articles about C₂₅H₃₃N₅O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 646-07-1
4-Methylpentanoic acid

: C₁₉H₂₃N₅O₂*2ClH

: 1246520-22-8
C₂₅H₃₃N₅O₃

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In chloroform; N,N-dimethyl-formamide; at 20 ℃; for 7h;

Reference yield:

: 117007-52-0
3-iodo-1H-pyrazolo[3,4-b]pyridine

: 1246520-22-8
C₂₅H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice

1.2: 1 h / 20 °C / Cooling with ice

2.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere

3.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice

3.2: Cooling with ice

4.1: trifluoroacetic acid / 16 h / Reflux

5.1: hydrogen / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 3 h / 20 °C

6.1: N-chloro-succinimide; triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C

6.2: Reflux

7.1: hydrogenchloride; methanol / ethyl acetate; chloroform / 28 h / 20 °C

8.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; chloroform / 7 h / 20 °C

With hydrogenchloride; methanol; N-chloro-succinimide; water; hydrogen; sodium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; sodium hydroxide; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 36404-88-3
2-chloro-3-carbaldehydepyridine

: 1246520-22-8
C₂₅H₃₃N₅O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: toluene-4-sulfonic acid; hydrazine hydrate / 21 h / 120 °C / Cooling with ice

2.1: potassium hydroxide; iodine / N,N-dimethyl-formamide / 1 h / 20 °C / Cooling with ice

3.1: sodium hydride / N,N-dimethyl-formamide / 3 h / Cooling with ice

3.2: 1 h / 20 °C / Cooling with ice

4.1: triethylamine / triphenylphosphine; palladium diacetate / 1,4-dioxane / 4 h / 100 °C / Inert atmosphere

5.1: sodium hydroxide; water / ethanol; tetrahydrofuran / 2 h / 20 °C / Cooling with ice

5.2: Cooling with ice

6.1: trifluoroacetic acid / 16 h / Reflux

7.1: hydrogen / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 3 h / 20 °C

8.1: N-chloro-succinimide; triphenylphosphine / tetrahydrofuran / 0.03 h / 20 °C

8.2: Reflux

9.1: hydrogenchloride; methanol / ethyl acetate; chloroform / 28 h / 20 °C

10.1: triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide; chloroform / 7 h / 20 °C

With hydrogenchloride; methanol; N-chloro-succinimide; water; hydrogen; iodine; sodium hydride; benzotriazol-1-ol; toluene-4-sulfonic acid; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; trifluoroacetic acid; potassium hydroxide; sodium hydroxide; palladium 10% on activated carbon; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; chloroform; water; ethyl acetate; N,N-dimethyl-formamide;