7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol

Base Information

Chemical Name:7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol
CAS No.:79754-54-4
Molecular Formula:C₁₇H₁₈O₃
Molecular Weight:270.328
Hs Code.:

Synonyms:7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol

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Chemical Property of 7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol

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Technology Process of 7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol

There total 18 articles about 7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 79754-58-8
7-hydroxy-4-p-hydroxybenzyl-3,4-dihydronaphthalen-1(2H)-one

: 79754-54-4
7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol

Guidance literature:: With sodium tetrahydroborate; In ethanol;
DOI:10.1039/P19810002662

Reference yield:

: 6443-74-9
p-methoxy-α-p-methoxyphenylcinnamonitrile

: 79754-54-4
7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol

Guidance literature:: Multi-step reaction with 6 steps

1: 21 percent / dry hydrogen chloride / tin(II) chloride / diethyl ether / 6 h

2: 20 percent / piperidine / pyridine / 1.) steam-bath, 10 h, 2.) reflux, 4 h

3: 63 percent / aq. sodium hydroxide, nickel-aluminium alloy / 2 h / 80 °C

4: 84 percent / polyphosphoric acid / 1.5 h / 85 °C

5: 76 percent / 48percent hydrobromic acid / acetic acid / 6 h / Heating

6: 90 percent / sodium borohydride / ethanol

With piperidine; hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; PPA; nickel-aluminium alloy; hydrogen bromide; tin(ll) chloride; In pyridine; diethyl ether; ethanol; acetic acid;
DOI:10.1039/P19810002662

Reference yield:

: 79754-49-7
3-hydroxy-3,4-bis-(4-methoxy-phenyl)-butyric acid ethyl ester

: 79754-54-4
7-hydroxy-4-p-hydroxybenzyl-1,2,3,4-tetrahydro-1-naphthol

Guidance literature:: Multi-step reaction with 8 steps

1: perchloric acid, hydrogen / 10percent palladium-carbon / acetic acid / 17 h / 735.5 Torr

2: ethanolic potassium hydroxide / H₂O

3: thionyl chloride

4: diethyl ether / 0 °C

5: silver oxide, aq. sodium thiosulphate / dioxane / 2 h / 65 - 70 °C

6: 84 percent / polyphosphoric acid / 1.5 h / 85 °C

7: 76 percent / 48percent hydrobromic acid / acetic acid / 6 h / Heating

8: 90 percent / sodium borohydride / ethanol

With potassium hydroxide; sodium tetrahydroborate; thionyl chloride; perchloric acid; PPA; hydrogen bromide; hydrogen; sodium thiosulfate; silver(l) oxide; palladium on activated charcoal; In 1,4-dioxane; diethyl ether; ethanol; water; acetic acid;
DOI:10.1039/P19810002662