1,2-Bis(4-methoxyphenyl)prop-2-en-1-one

Base Information

• Chemical Name: 1,2-Bis(4-methoxyphenyl)prop-2-en-1-one
• CAS No.: 67295-38-9
• Molecular Formula: C17H16O3
• Molecular Weight: 268.312
• DSSTox Substance ID: DTXSID00529387
• Wikidata: Q82399778

Synonyms:1,2-Bis(4-methoxyphenyl)prop-2-en-1-one;67295-38-9;SCHEMBL18982976;DTXSID00529387

Chemical Property of 1,2-Bis(4-methoxyphenyl)prop-2-en-1-one

Chemical Property:

• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 5
• Exact Mass: 268.109944368
• Heavy Atom Count: 20
• Complexity: 334

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C=C1)C(=C)C(=O)C2=CC=C(C=C2)OC

Technology Process of 1,2-Bis(4-methoxyphenyl)prop-2-en-1-one

There total 11 articles about 1,2-Bis(4-methoxyphenyl)prop-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

1,4-di(4-methoxyphenyl)ethanone (120-44-5) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 1, 2-bis(4-methoxyphenyl)prop-2-en-1-one (67295-38-9)

Guidance literature:

With dipotassium peroxodisulfate; copper (II) trifluoroacetate hydrate; at 100 ℃; for 24h; Schlenk technique; Inert atmosphere;

DOI:10.1039/c4cc02275k

Reference yield: 77.0%

4-Methoxystyrene (637-69-4,24936-44-5) + 4-methoxy-benzaldehyde (123-11-5) → 1, 2-bis(4-methoxyphenyl)prop-2-en-1-one (67295-38-9)

Guidance literature:

With tris(bipyridine)ruthenium(II) dichloride hexahydrate; 3-(2,6-diisopropylphenyl)-5,6,7,8-tetrahydro-4H-cyclohepta[d]thiazol-3-ium perchlorate; 3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone; sodium benzenesulfonate; potassium carbonate; In dimethyl sulfoxide; at 20 ℃; Irradiation;

DOI:10.1021/acscatal.1c02890

Reference yield: 57.0%

1,2-bis-(4-methoxy-phenyl)-propan-1-one (35258-41-4) → 1, 2-bis(4-methoxyphenyl)prop-2-en-1-one (67295-38-9) + 2-bromo-1,2-bis(4-methoxyphenyl)propan-1-one + 1-(4-methoxyphenyl)ethanone (100-06-1)

Guidance literature:

With oxygen; copper(ll) bromide; In acetonitrile; at 85 ℃; for 132h; Sealed tube; Microwave irradiation;

upstream raw materials:

formaldehyd

1,4-di(4-methoxyphenyl)ethanone

3-benzylsulfanyl-1,2-bis-(4-methoxy-phenyl)-propan-1-one

[2,3-bis-(4-methoxy-phenyl)-3-oxo-propyl]-trimethyl-ammonium; iodide

Downstream raw materials:

1,2-bis-(4-methoxy-phenyl)-pentan-1-one

3-(tert-Butyl-hydroxy-amino)-1,2-bis-(4-methoxy-phenyl)-propan-1-one

1,2-bis(4'-methoxyphenyl)-4-methyl-4-nitropentan-1-one

2,3-bis(4'-methoxyphenyl)-5,5-dimethyl-1-pyrroline 1-oxide

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