Technology Process of C24H23NO6*ClH
There total 6 articles about C24H23NO6*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol;
at 20 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: tert.-butyl lithium / hexane / 0.75 h / -78 °C
1.2: 12 h
1.3: pH 7 - 8
2.1: toluene-4-sulfonic acid / dichloromethane / 3 h / 20 °C
3.1: methanol; potassium carbonate / 12 h / 20 °C
4.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C
5.1: hydrogenchloride / methanol / 12 h / 20 °C
With
hydrogenchloride; methanol; dmap; tert.-butyl lithium; potassium carbonate; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; hexane; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C
2: hydrogenchloride / methanol / 12 h / 20 °C
With
hydrogenchloride; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
methanol; dichloromethane;