(1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

Base Information

Chemical Name:(1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene
CAS No.:476350-47-7
Molecular Formula:C₂₄H₃₂O₅S
Molecular Weight:432.581
Hs Code.:

Synonyms:(1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

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Chemical Property of (1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

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Technology Process of (1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

There total 1 articles about (1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116511-95-6
(benzenesulfonyl)methyllithium

: 3536-96-7
vinylmagnesium chloride

: 107-30-2
chloromethyl methyl ether

: 74-88-4
methyl iodide

: 476350-47-7
(1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

Guidance literature:: Multistep reaction.;
DOI:10.1021/ol026827a

Reference yield: 61.0%

: 870-63-3
prenyl bromide

: 476350-47-7
(1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

: (1S,2'R,3'S,4R)-1-(3'-phenylsulfonyl-6'-methyl-hept-5'-en-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

: (1S,2'R,3'R,4R)-1-(3'-phenylsulfonyl-6'-methyl-hept-5'-en-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene

Guidance literature:: (1S,2R',4R)-1-(1'-phenylsulfonyl-prop-2'-yl)-5,6-dimethoxy-4-methoxymethyl-7-methyl-1,2,3,4-tetrahydro-naphthalene; With n-butyllithium; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; hexane; at -78 ℃; for 1.5h;

prenyl bromide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 0.25h; Further stages.;
DOI:10.1021/ol026827a