5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane

Base Information

• Chemical Name: 5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane
• CAS No.: 177161-89-6
• Molecular Formula: C₂₉H₃₃F₁₇O₃
• Molecular Weight: 752.552

Synonyms:5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane

Chemical Property of 5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane

Chemical Property:

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Technology Process of 5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane

There total 2 articles about 5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluorononadecanol (1512-02-3) → 5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane (177161-89-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / pyridine / 5 h / -15 °C

2: 1.) NaH / 1.) THF, 4 h, room t. and 65 deg C, 45 min, 2.) THF, 3 days, reflux

With pyridine; sodium hydride;

DOI:10.1002/hlca.19960790209

Reference yield:

Methanesulfonic acid 12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyl ester (177161-62-5) + 2-phenyl-[1,3]dioxan-5-ol (1708-40-3) → 5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane (177161-89-6)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, 4 h, room t. and 65 deg C, 45 min, 2.) THF, 3 days, reflux;

DOI:10.1002/hlca.19960790209

Reference yield: 70.0%

5-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-2-phenyl-[1,3]dioxane (177161-89-6) → 3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol (177161-90-9)

Guidance literature:

With tetrahydrofuran; borane; In tetrahydrofuran; at 40 - 45 ℃; for 60h;

DOI:10.1002/hlca.19960790209

upstream raw materials:

Methanesulfonic acid 12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyl ester

2-phenyl-[1,3]dioxan-5-ol

12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluorononadecanol

Downstream raw materials:

3-Benzyloxy-2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-heptadecafluoro-nonadecyloxy)-propan-1-ol

[2-(12,12,13,13,14,14,15,15,16,16,17,17,18,18,19,19,19-Heptadecafluoro-nonadecyloxy)-3-(12,12,13,13,14,14,15,15,15-nonafluoro-pentadecyloxy)-propoxymethyl]-benzene

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