Technology Process of C12H8FN3O
There total 6 articles about C12H8FN3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
for 12h;
Inert atmosphere;
Cooling;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium acetate / ethanol; water / 18 h / 50 °C
2: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / 1-methyl-pyrrolidin-2-one / 18 h / 120 °C
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 61 h
With
sodium acetate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium acetate / ethanol; water / 18 h / 50 °C
2: potassium carbonate / cis-N,N'-dimethyl-1,2-diaminocyclohexane; copper(l) iodide / 1-methyl-pyrrolidin-2-one / 18 h / 120 °C
3: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 61 h
With
sodium acetate; potassium carbonate; 3-chloro-benzenecarboperoxoic acid;
copper(l) iodide; cis-N,N'-dimethyl-1,2-diaminocyclohexane;
In
1-methyl-pyrrolidin-2-one; ethanol; dichloromethane; water;