3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

Base Information

Chemical Name:3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate
CAS No.:1196996-64-1
Molecular Formula:C₃₅H₃₅NO₆
Molecular Weight:565.666
Hs Code.:

Synonyms:3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

Suppliers and Price of 3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

There total 13 articles about 3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1196996-63-0
6-((4-(benzyloxy-3-methoxyphenethyl)carbamoyl)methyl)-3-(benzyloxy)-2-methoxybenzyl acetate

: 1196996-64-1
3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

Guidance literature:: With trichlorophosphate; In acetonitrile; for 2h; Inert atmosphere; Reflux;
DOI:10.1021/jo9020826

Reference yield:

: 22231-61-4
2-[4-(benzyloxy)-3-methoxyphenyl]ethylamine

: 1196996-64-1
3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 14 h / Reflux

2: pyridine / dichloromethane / 1.5 h / 0 - 20 °C

3: trichlorophosphate / acetonitrile / 1 h / Reflux; Inert atmosphere

With pyridine; trichlorophosphate; In ethanol; dichloromethane; acetonitrile; 3: |Bischler-Napieralski Reaction;
DOI:10.1016/j.bmc.2012.12.016

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 1196996-64-1
3-(benzyloxy)-6-((7-(benzyloxy)-3,4-dihydro-6-methoxyisoquinolin-1-yl)methyl)-2-methoxybenzyl acetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetic acid; bromine / 2 h / 20 °C

2.1: potassium carbonate / acetone / Reflux

3.1: potassium hydroxide; water; copper; copper(II) oxide / 1 h / 140 °C / Inert atmosphere; Microwave irradiation

4.1: phenylboronic acid / toluene / 1 h / Reflux; Dean-Stark

4.2: 46 h / 100 °C / Molecular sieve; Sealed tube

4.3: 2 h / Reflux

5.1: potassium carbonate / acetone / 4 h / Reflux

6.1: ethanol / 14 h / Reflux

7.1: pyridine / dichloromethane / 1.5 h / 0 - 20 °C

8.1: trichlorophosphate / acetonitrile / 1 h / Reflux; Inert atmosphere

With pyridine; water; bromine; copper; potassium carbonate; acetic acid; copper(II) oxide; potassium hydroxide; trichlorophosphate; phenylboronic acid; In ethanol; dichloromethane; acetone; toluene; acetonitrile; 8.1: |Bischler-Napieralski Reaction;
DOI:10.1016/j.bmc.2012.12.016