N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide

Base Information

• Chemical Name: N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide
• CAS No.: 1040191-39-6
• Molecular Formula: C₂₃H₃₆N₄O₁₂S
• Molecular Weight: 592.624
• Mol file: 1040191-39-6.mol

Synonyms:N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide

Chemical Property of N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide

There total 1 articles about N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N,N'-diacetylchitobiose (14200-67-0,18422-28-1,34147-27-8,35991-83-4,109957-89-3,109957-93-9,119719-43-6,125760-94-3,141725-02-2,145841-62-9,148682-80-8) + toluene-4-sulfonic acid hydrazide (1576-35-8) → N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide (1040191-39-6)

Guidance literature:

With acetic acid; In N,N-dimethyl-formamide; at 37 ℃; for 48h;

DOI:10.1021/ol801232f

Reference yield:

methanol (67-56-1) + N'-(2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-β-glucopyranoside)-p-toluenesulfono-hydrazide (1040191-39-6) → methyl-N,N'-diacetyl-β-chitobioside (136198-40-8,141989-69-7,19272-54-9,21217-11-8) + methyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-α-glucopyranoside (21217-11-8)

Guidance literature:

With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; optical yield given as %de;

DOI:10.1021/ol801232f

upstream raw materials:

N,N'-diacetylchitobiose

toluene-4-sulfonic acid hydrazide

Downstream raw materials:

methyl-N,N'-diacetyl-β-chitobioside

methyl 2-acetamido-4-O-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-2-deoxy-D-α-glucopyranoside