N-benzylmeroquinene alcohol

Base Information

Chemical Name:N-benzylmeroquinene alcohol
CAS No.:134261-48-6
Molecular Formula:C₁₆H₂₃NO
Molecular Weight:245.365
Hs Code.:

Synonyms:N-benzylmeroquinene alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzylmeroquinene alcohol

Chemical Property:

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Technology Process of N-benzylmeroquinene alcohol

There total 9 articles about N-benzylmeroquinene alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 134261-56-6
((3R,4S)-1-Benzyl-2-oxo-3-vinyl-piperidin-4-yl)-acetic acid methyl ester

: 134261-48-6
N-benzylmeroquinene alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/jo00015a036

Reference yield:

: 134261-49-7
N-benzyl-2-(1,3-dioxolan-2-yl)ethanamine

: 134261-48-6
N-benzylmeroquinene alcohol

Guidance literature:: Multi-step reaction with 8 steps

1: 1) Et₃N / 1) CH₂Cl₂, 0 deg C, 5 min, 2) CH₂Cl₂, warm to r.t.

2: 30percent HCl / tetrahydrofuran / 42 h / Ambient temperature

3: 64 percent / tetrahydrofuran / 14 h / Heating

4: 1) Et₃N / 1) CH₂Cl₂, r.t., 5 min, 2) CH₂Cl₂, 5 min

5: 87 percent / KF*2H₂O / methanol / 2 h / Heating

6: 86 percent / m-CPBA, aq.Na₂HPO₄ / CH₂Cl₂ / 39 h / Ambient temperature

7: 71 percent / conc.HCl / 24 h / Ambient temperature

8: 97 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

With hydrogenchloride; potassium fluoride; disodium hydrogenphosphate; lithium aluminium tetrahydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo00015a036

Reference yield:

: 134261-59-9
(E)-N-Benzyl-N-(3-oxo-propyl)-3-trimethylsilanyl-acrylamide

: 134261-48-6
N-benzylmeroquinene alcohol

Guidance literature:: Multi-step reaction with 6 steps

1: 64 percent / tetrahydrofuran / 14 h / Heating

2: 1) Et₃N / 1) CH₂Cl₂, r.t., 5 min, 2) CH₂Cl₂, 5 min

3: 87 percent / KF*2H₂O / methanol / 2 h / Heating

4: 86 percent / m-CPBA, aq.Na₂HPO₄ / CH₂Cl₂ / 39 h / Ambient temperature

5: 71 percent / conc.HCl / 24 h / Ambient temperature

6: 97 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

With hydrogenchloride; potassium fluoride; disodium hydrogenphosphate; lithium aluminium tetrahydride; triethylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jo00015a036