2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

Base Information

Chemical Name:2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile
CAS No.:77715-28-7
Molecular Formula:C₃₀H₂₉NO₅
Molecular Weight:483.564
Hs Code.:

Synonyms:2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

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Chemical Property of 2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

Chemical Property:

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Technology Process of 2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

There total 1 articles about 2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77668-04-3
2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

: 109-94-4
formic acid ethyl ester

: 77715-28-7
2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

Guidance literature:: With sodium hydride; In diethyl ether; ethanol; for 15h;

Reference yield: 80.0%

: 77715-28-7
2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

: 79-19-6
thiosemicarbazide

: 92949-41-2,92999-91-2
2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile thiosemicarbazone

Guidance literature:: In ethanol; acetic acid; at 55 - 60 ℃; for 0.5h;

Reference yield:

: 77715-28-7
2-formyl-2-(2,3-O-isopropylidene-5-O-trityl-D-ribofuranosyl)acetonitrile

: 76-84-6
triphenylmethyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / aq. ethanol; acetic acid / 0.5 h / 55 - 60 °C

2: 760 mg / 1.) 1 M sodium ethoxide; 2.) acetic acid / ethanol / 0.25 h / Ambient temperature

3: 64 percent / 6 h / 85 - 90 °C

4: 10percent HCl / methanol / 0.17 h / Ambient temperature

With hydrogenchloride; sodium ethanolate; acetic acid; In methanol; ethanol; acetic acid;