N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine

Base Information

Chemical Name:N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine
CAS No.:877128-47-7
Molecular Formula:C₂₉H₄₆INO₃Si₂
Molecular Weight:639.765
Hs Code.:

Synonyms:N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine

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Technology Process of N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine

There total 6 articles about N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.3%

: 877128-45-5
2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]-N-methylethylamine

: 70-11-1
α-bromoacetophenone

: 877128-47-7
N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine

Guidance literature:: With methyloxirane; In 1,4-dioxane; at 105 ℃; for 2h;
DOI:10.3987/COM-05-10554

Reference yield:

: 877128-41-1
2-[3,4-di(t-butyldimethylsilyloxy)phenyl]-N-formylethylamine

: 877128-47-7
N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 94.4 percent / iodine; silver trifluoroacetate / CHCl₃ / 0.25 h / 20 °C

2: 32.7 percent / BH₃ / tetrahydrofuran / 1 h / Heating

3: 85.3 percent / propylene oxide / dioxane / 2 h / 105 °C

With borane; iodine; silver trifluoroacetate; methyloxirane; In tetrahydrofuran; 1,4-dioxane; chloroform;
DOI:10.3987/COM-05-10554

Reference yield:

: 877128-43-3
2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]-N-formylethylamine

: 877128-47-7
N-{2-[4,5-di(t-butyldimethylsilyloxy)-2-iodophenyl]ethyl}-N-methylphenacylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 32.7 percent / BH₃ / tetrahydrofuran / 1 h / Heating

2: 85.3 percent / propylene oxide / dioxane / 2 h / 105 °C

With borane; methyloxirane; In tetrahydrofuran; 1,4-dioxane;
DOI:10.3987/COM-05-10554