(5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one)

Base Information

• Chemical Name: (5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one)
• CAS No.: 916747-72-3
• Molecular Formula: C₃₂H₂₄N₆O₂S₂
• Molecular Weight: 588.714
• Mol file: 916747-72-3.mol

Synonyms:(5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one)

Chemical Property of (5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one)

There total 1 articles about (5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

3-phenyl-(5Z)-5-(pyridine-2-ylmethylene)-2-thioxoimidazolin-4-one (145693-89-6) + ethylene dibromide (106-93-4) → (5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one) (916747-72-3)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at -10 - 20 ℃; for 4h;

DOI:10.1007/s11172-006-0092-7

Reference yield: 65.0%

(5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one) (916747-72-3) + cobalt(II) chloride hexahydrate → (5Z,5'Z)-2.2'-(ethane-1,2-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)dicobalt(II) tetrachloride (916747-79-0)

Guidance literature:

In ethanol; dichloromethane; EtOH was carefully added to soln. of ligand in CH2Cl2; soln. of Co salt in EtOH was slowly added; mixt. was tightly closed and kept until ppt. was formed; ppt. filtered off; dried (air); elem. anal.;

DOI:10.1007/s11172-006-0092-7

Reference yield: 55.0%

(5Z,5'Z)-2,2'-(ethane-1,2-diyldisulfanyldiyl)bis(5-(pyridine-2-ylmethylene)-3-phenyl-3,5-dihydro-4H-imidazole-4-one) (916747-72-3) + copper(II) choride dihydrate → C32H24Cl3Cu2N6O2S2

Guidance literature:

In dichloromethane;

DOI:10.1021/jm500154f

upstream raw materials:

3-phenyl-(5Z)-5-(pyridine-2-ylmethylene)-2-thioxoimidazolin-4-one

ethylene dibromide

Downstream raw materials:

(5Z,5'Z)-2.2'-(ethane-1,2-diyldisulfanyldiyl)bis(3-phenyl-5-(2-pyridylmethylene)-3,5-dihydro-4H-imidazol-4-one)dicobalt(II) tetrachloride