(S)-3-Methylheptyl benzyl ether

Base Information

Chemical Name:(S)-3-Methylheptyl benzyl ether
CAS No.:84184-37-2
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:

Synonyms:(S)-3-Methylheptyl benzyl ether

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Chemical Property of (S)-3-Methylheptyl benzyl ether

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Technology Process of (S)-3-Methylheptyl benzyl ether

There total 9 articles about (S)-3-Methylheptyl benzyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 75-16-1
methylmagnesium bromide

: (S)-6-benzyloxy-4-methylhexyl tosylate

: 84184-37-2
(S)-3-Methylheptyl benzyl ether

Guidance literature:: With dilithium tetrachlorocuprate; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2015.04.107

Reference yield: 55.0%

: 84184-35-0
Benzyl 3-tosyloxybutyl ether

: 84184-37-2
(S)-3-Methylheptyl benzyl ether

Guidance literature:: In diethyl ether; at -70 ℃; for 12h;
DOI:10.1055/s-1982-29930

Reference yield:

: 7540-51-4
(S)-3,7-dimethyl-6-octen-1-ol

: 84184-37-2
(S)-3-Methylheptyl benzyl ether

Guidance literature:: Multi-step reaction with 6 steps

1: potassium tert-butylate / dimethyl sulfoxide; benzene / 1.25 h

2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tert-butyl alcohol; water; acetone / 96 h / 20 °C

3: periodic acid dihydrate / 0.5 h / 5 - 10 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 - 5 °C

5: dmap; pyridine / 1.5 h / 0 - 5 °C

6: dilithium tetrachlorocuprate / tetrahydrofuran; diethyl ether / -78 - 20 °C / Inert atmosphere

With pyridine; dmap; osmium(VIII) oxide; lithium aluminium tetrahydride; periodic acid dihydrate; dilithium tetrachlorocuprate; potassium tert-butylate; 4-methylmorpholine N-oxide; In tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide; acetone; tert-butyl alcohol; benzene;
DOI:10.1016/j.tet.2015.04.107