<2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester

Base Information

Chemical Name:<2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester
CAS No.:172756-79-5
Molecular Formula:C₁₅H₂₁IN₂O₅
Molecular Weight:436.247
Hs Code.:

Synonyms:<2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester

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Chemical Property of <2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester

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Technology Process of <2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester

There total 6 articles about <2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 172756-78-4
Methanesulfonic acid 2-[2-tert-butoxycarbonylamino-1-(2-nitro-phenyl)-ethoxy]-ethyl ester

: 172756-79-5
<2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester

Guidance literature:: With sodium iodide; In acetone; for 2h; Heating;
DOI:10.1021/jo951190c

Reference yield:

: 48140-35-8
2-(2-nitrophenyl)-1,3-dioxolane

: 172756-79-5
<2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / ZnI₂ / 0.25 h / Ambient temperature

2: 1.) BH₃*THF, 2.) 6N HCl / 1.) 25 deg C, 4 h

3: 98 percent / Et₃N / tetrahydrofuran / 0.75 h / Ambient temperature

4: 95 percent / Et₃N / diethyl ether / 1 h / 25 °C

5: 98 percent / NaI / acetone / 2 h / Heating

With hydrogenchloride; borane-THF; triethylamine; sodium iodide; zinc(II) iodide; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1021/jo951190c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 172756-79-5
<2-(2-iodoethoxy)-2-(2-nitrophenyl)ethyl>carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / Et₃N / tetrahydrofuran / 0.75 h / Ambient temperature

2: 95 percent / Et₃N / diethyl ether / 1 h / 25 °C

3: 98 percent / NaI / acetone / 2 h / Heating

With triethylamine; sodium iodide; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1021/jo951190c