rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene

Base Information

Chemical Name:rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene
CAS No.:130970-85-3
Molecular Formula:C₂₈H₃₀O₃
Molecular Weight:414.544
Hs Code.:

Synonyms:rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene

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Chemical Property of rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene

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Technology Process of rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene

There total 4 articles about rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 100-39-0
benzyl bromide

: 130970-84-2,143058-81-5
DL-(1,3/2)-1,2-dihydroxy-3-hydroxymethyl-5-cyclohexene

: 130970-85-3
rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(90)84020-U

Reference yield:

: 74766-78-2,96291-86-0,115225-42-8
3,4-di-O-acetyl-1,5-anhydro-6-bromo-2,6-dideoxy-5a-carba-DL-arabino-hex-1-enitol

: 130970-85-3
rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide; H₂O / 4 h / 100 °C

2: methanolic NaOMe / 2 h / Ambient temperature

3: 1.) NaH / 1.) N,N-dimethylformamide, 0 deg C, 30 min, 2.) room temperature, 3 h

With sodium methylate; sodium hydride; In water; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)80074-D

Reference yield:

: 104731-67-1,108867-01-2,108867-02-3
DL-(1,3/2)-2,3-Diacetoxy-4-cyclohexene-1-carboxylic acid

: 130970-85-3
rac-((((1R,2R,6R)-6-((benzyloxy)methyl)cyclohex-3-ene-1,2-diyl)bis-(oxy))bis(methylene))dibenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) LiAlH₄, 2.) pyridine / 1.) THF, room temperature, 1.5 h, 2.) room temperature, 2 h

2: methanolic NaOMe / 2 h / Ambient temperature

3: 1.) NaH / 1.) N,N-dimethylformamide, 0 deg C, 30 min, 2.) room temperature, 3 h

With pyridine; lithium aluminium tetrahydride; sodium methylate; sodium hydride;
DOI:10.1016/0008-6215(90)80074-D