2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole

Base Information

Chemical Name:2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole
CAS No.:1186610-87-6
Molecular Formula:C₂₅H₂₉BrN₂O₄S
Molecular Weight:533.486
Hs Code.:

Synonyms:2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole

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Technology Process of 2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole

There total 1 articles about 2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 89796-20-3
N-(2-bromoprop-2-enyl)-N-butylamine

: 1186610-45-6
2-ethynyl-4-(methoxycarbonyl)-N-(p-toluenesulfonyl)aniline

: 1186610-87-6
2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole

Guidance literature:: With copper(I) bromide; In 1,4-dioxane; at 80 ℃; for 3h; Inert atmosphere;
DOI:10.1021/jo901328q

Reference yield: 54.0%

: 1186610-87-6
2-{(N-(2-bromoprop-2-en-1-yl)-N-butylamino)methyl}-5-(methoxycarbonyl)-1-tosylindole

: 1186610-99-0
2-butyl-4-methylene-9-tosyl-6-(methoxycarbonyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Guidance literature:: With cesium acetate; palladium diacetate; triphenylphosphine; In 2,4-dichlorophenoxyacetic acid dimethylamine; at 100 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/jo901328q