6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

Base Information

Chemical Name:6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin
CAS No.:1284217-06-6
Molecular Formula:C₆₀H₇₁N₉O₂₂
Molecular Weight:1270.27
Hs Code.:

Synonyms:6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

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Chemical Property of 6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

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Technology Process of 6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

There total 1 articles about 6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 1284217-05-5
6'-azido-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

: 40371-50-4
S-4-benzyloxycarbonylamino-2-hydroxybutyric acid

: 1284217-06-6
6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

Guidance literature:: S-4-benzyloxycarbonylamino-2-hydroxybutyric acid; With 1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 2h;

6'-azido-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin; In tetrahydrofuran;

With water; ammonium chloride; In tetrahydrofuran;

Reference yield: 85.0%

: 1284217-06-6
6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

: 20194-18-7
sodium phenyl-methanolate

: 1284217-07-7
6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-3,2',2''',6'''-tetra-N-Cbz-4',5'-dehydro-3'-deoxyneomycin

Guidance literature:: 6'-azido-1-(N-Cbz-2(S)-hydroxy-4-aminobutyryl)-4''',6'''-carbamate-3,2',2'''-tri-N-Cbz-4',5'-dehydro-3'-deoxyneomycin; sodium phenyl-methanolate; In benzyl alcohol; for 16h;

With acetic acid; In benzyl alcohol;