C₇H₄BrClINO

Base Information

Chemical Name:C₇H₄BrClINO
CAS No.:1357614-72-2
Molecular Formula:C₇H₄BrClINO
Molecular Weight:360.376
Hs Code.:

Synonyms:C₇H₄BrClINO

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Chemical Property of C₇H₄BrClINO

Chemical Property:

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Technology Process of C₇H₄BrClINO

There total 5 articles about C₇H₄BrClINO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1357614-70-0
(E/Z)-3-bromo-4-iodobenzaldehyde oxime

: 1357614-72-2
C₇H₄BrClINO

Guidance literature:: With N-chloro-succinimide; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

Reference yield:

: 873387-82-7
3-bromo-4-iodobenzaldehyde

: 1357614-72-2
C₇H₄BrClINO

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride / water; ethanol / 19 h / 20 - 50 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 18 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: 249647-24-3
3-bromo-4-iodobenzoic acid methyl ester

: 1357614-72-2
C₇H₄BrClINO

Guidance literature:: Multi-step reaction with 4 steps

1.1: diisobutylaluminium hydride / dichloromethane / -78 - 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C

2.1: sodium hydrogencarbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / water; dichloromethane / 0 - 20 °C

3.1: hydroxylamine hydrochloride / water; ethanol / 19 h / 20 - 50 °C

4.1: N-chloro-succinimide / N,N-dimethyl-formamide / 18 h / 20 °C

With sodium hypochlorite; N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydroxylamine hydrochloride; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium bromide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;