(E/Z)-3-bromo-4-iodobenzaldehyde oxime

Base Information

Chemical Name:(E/Z)-3-bromo-4-iodobenzaldehyde oxime
CAS No.:1357614-70-0
Molecular Formula:C₇H₅BrINO
Molecular Weight:325.931
Hs Code.:

Synonyms:(E/Z)-3-bromo-4-iodobenzaldehyde oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E/Z)-3-bromo-4-iodobenzaldehyde oxime

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Technology Process of (E/Z)-3-bromo-4-iodobenzaldehyde oxime

There total 4 articles about (E/Z)-3-bromo-4-iodobenzaldehyde oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 873387-82-7
3-bromo-4-iodobenzaldehyde

: 1357614-70-0
(E/Z)-3-bromo-4-iodobenzaldehyde oxime

Guidance literature:: With hydroxylamine hydrochloride; In ethanol; water; at 20 - 50 ℃; for 19h;

Reference yield:

: 249647-24-3
3-bromo-4-iodobenzoic acid methyl ester

: 1357614-70-0
(E/Z)-3-bromo-4-iodobenzaldehyde oxime

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / dichloromethane / -78 - 20 °C / Inert atmosphere

1.2: 0.5 h / 20 °C

2.1: sodium hydrogencarbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / water; dichloromethane / 0 - 20 °C

3.1: hydroxylamine hydrochloride / water; ethanol / 19 h / 20 - 50 °C

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydroxylamine hydrochloride; diisobutylaluminium hydride; sodium hydrogencarbonate; sodium bromide; In ethanol; dichloromethane; water;

Reference yield:

: 249647-26-5
(3-bromo-4-iodophenyl)methanol

: 1357614-70-0
(E/Z)-3-bromo-4-iodobenzaldehyde oxime

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; sodium bromide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hypochlorite / water; dichloromethane / 0 - 20 °C

2: hydroxylamine hydrochloride / water; ethanol / 19 h / 20 - 50 °C

With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydroxylamine hydrochloride; sodium hydrogencarbonate; sodium bromide; In ethanol; dichloromethane; water;