1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

Base Information

Chemical Name:1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene
CAS No.:144582-00-3
Molecular Formula:C₄₄H₅₁N₃O₅
Molecular Weight:701.906
Hs Code.:

Synonyms:1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

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Chemical Property of 1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

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Technology Process of 1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

There total 15 articles about 1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 144581-98-6
1,4-Bis<4-(5-ethoxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

: 100-51-6,185532-71-2
benzyl alcohol

: 144582-00-3
1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

Guidance literature:: With sodium phenyl-methanolate; at 100 ℃; for 0.5h; under 12 Torr;

Reference yield:

: 19417-59-5
1,4-bis-(3-bromopropyl)-benzene

: 144582-00-3
1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

Guidance literature:: Multi-step reaction with 10 steps

1: ethanol

2: aq. KOH

3: TsOH / toluene

4: NaNO₂, CF₃CO₂H

5: aq. KOH

6: SOCl₂ / Heating

7: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

8: B₂H₆ / tetrahydrofuran

9: 90 percent / H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

10: 75 percent / PhCH₂ONa / 0.5 h / 100 °C / 12 Torr

With potassium hydroxide; thionyl chloride; hydrogen; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; toluene;

Reference yield:

: 19417-58-4
[1,4-phenylene]-bis(3-hydroxypropane)

: 144582-00-3
1,4-Bis<4-(5-benzyloxycarbonyl-2,4-dimethylpyrrol-3-yl)butyl>-2-acetamidobenzene

Guidance literature:: Multi-step reaction with 11 steps

1: HBr

2: ethanol

3: aq. KOH

4: TsOH / toluene

5: NaNO₂, CF₃CO₂H

6: aq. KOH

7: SOCl₂ / Heating

8: SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

9: B₂H₆ / tetrahydrofuran

10: 90 percent / H₂, NaOAc / 10percent Pd/C / tetrahydrofuran / 760 Torr

11: 75 percent / PhCH₂ONa / 0.5 h / 100 °C / 12 Torr

With potassium hydroxide; thionyl chloride; hydrogen bromide; hydrogen; sodium acetate; tin(IV) chloride; toluene-4-sulfonic acid; sodium phenyl-methanolate; trifluoroacetic acid; diborane; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; toluene;