1-PHENYL-1'H-3,3'-DIMETHYL-5-DIMETHYL-5-HYDROXY[4,5']-BIPYRAZOL

Base Information

Chemical Name:1-PHENYL-1'H-3,3'-DIMETHYL-5-DIMETHYL-5-HYDROXY[4,5']-BIPYRAZOL
CAS No.:168848-22-4
Molecular Formula:C₁₄H₁₄N₄O
Molecular Weight:254.291
Hs Code.:
Mol file:168848-22-4.mol

Synonyms:5-hydroxy-3-methyl-1-phenyl-4-(3-methylpyrazol-5-yl)pyrazole

Suppliers and Price of 1-PHENYL-1'H-3,3'-DIMETHYL-5-DIMETHYL-5-HYDROXY[4,5']-BIPYRAZOL

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 1-PHENYL-1'H-3,3'-DIMETHYL-5-DIMETHYL-5-HYDROXY[4,5']-BIPYRAZOL

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-PHENYL-1'H-3,3'-DIMETHYL-5-DIMETHYL-5-HYDROXY[4,5']-BIPYRAZOL

There total 5 articles about 1-PHENYL-1'H-3,3'-DIMETHYL-5-DIMETHYL-5-HYDROXY[4,5']-BIPYRAZOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 87100-61-6
1-(5-hydroxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)butane-1,3-dione

: 168848-22-4
5-hydroxy-3-methyl-1-phenyl-4-(3-methylpyrazol-5-yl)pyrazole

Guidance literature:: With hydrazine hydrate; In ethanol; for 1.5h; Heating;
DOI:10.1002/jhet.5570360529

Reference yield:

: 771-03-9
3-acetyl-4-hydroxy-6-methyl-2H-pyran-2-one

: 168848-22-4
5-hydroxy-3-methyl-1-phenyl-4-(3-methylpyrazol-5-yl)pyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: benzene / Reflux

2: acetic acid / Reflux

3: hydrazine hydrate / ethanol / Reflux

With hydrazine hydrate; acetic acid; In ethanol; benzene;
DOI:10.1007/s00044-017-2071-y

Reference yield:

: 54107-17-4
3-(2-phenylhydrazonoethyl)-4-hydroxy-6-methylpyrone-2-one

: 168848-22-4
5-hydroxy-3-methyl-1-phenyl-4-(3-methylpyrazol-5-yl)pyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / Reflux

2: hydrazine hydrate / ethanol / Reflux

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1007/s00044-017-2071-y