1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid

Base Information

Chemical Name:1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid
CAS No.:13782-37-1
Molecular Formula:C₁₇H₁₈N₄O
Molecular Weight:294.356
Hs Code.:

Synonyms:1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid

Chemical Property:

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Technology Process of 1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid

There total 5 articles about 1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 13782-38-2
2,4-dimethylcarbonohydrazide

: 100-52-7
benzaldehyde

: 13782-37-1
1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid

Guidance literature:: In ethanol; Heating;

Reference yield: 85.0%

: 4114-25-4
1,5-dibenzylidenecarbonohydrazide

: 77-78-1
dimethyl sulfate

: 13782-37-1
1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 2h; Reflux;
DOI:10.1021/jo300027b

Reference yield:

: 100-52-7
benzaldehyde

: 13782-37-1
1,5-Dibenzyliden-2,4-dimethylcarbonohydrazid

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: sodium hydride / tetrahydrofuran / 2 h / Reflux

With sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1021/jo300027b