phenyl-N-phenyl(phenylthio)ketenimine

Base Information

• Chemical Name: phenyl-N-phenyl(phenylthio)ketenimine
• CAS No.: 79865-99-9
• Molecular Formula: C₂₀H₁₅NS
• Molecular Weight: 301.412
• Mol file: 79865-99-9.mol

Synonyms:phenyl-N-phenyl(phenylthio)ketenimine

Chemical Property of phenyl-N-phenyl(phenylthio)ketenimine

Chemical Property:

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Technology Process of phenyl-N-phenyl(phenylthio)ketenimine

There total 1 articles about phenyl-N-phenyl(phenylthio)ketenimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

diethylphosphonate (73778-49-1) + phenyl isocyanate (103-71-9) → phenyl-N-phenyl(phenylthio)ketenimine (79865-99-9)

Guidance literature:

With sodium hydride; In tetrahydrofuran; 1.) 40 deg C, 5.5 h, 2.) 1 h, room temperature;

DOI:10.1039/P19810002727

Reference yield: 95.0%

phenyl-N-phenyl(phenylthio)ketenimine (79865-99-9) → α-phenylthio(phenyl)acetanilide (67447-91-0)

Guidance literature:

With hydrogenchloride; In tetrahydrofuran; water; for 3h; Ambient temperature;

DOI:10.1039/P19810002727

upstream raw materials:

diethylphosphonate

phenyl isocyanate

Downstream raw materials:

α-phenylthio(phenyl)acetanilide

Refernces