3-Methyl-1-(2,6,6-trimethyl-cyclohexen-1-yl)-heptatrien-1,3,5-saeure-7-nitril

Base Information

Chemical Name:3-Methyl-1-(2,6,6-trimethyl-cyclohexen-1-yl)-heptatrien-1,3,5-saeure-7-nitril
CAS No.:58526-71-9
Molecular Formula:C₁₇H₂₃N
Molecular Weight:241.376
Hs Code.:

Synonyms:3-Methyl-1-(2,6,6-trimethyl-cyclohexen-1-yl)-heptatrien-1,3,5-saeure-7-nitril

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Chemical Property of 3-Methyl-1-(2,6,6-trimethyl-cyclohexen-1-yl)-heptatrien-1,3,5-saeure-7-nitril

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Technology Process of 3-Methyl-1-(2,6,6-trimethyl-cyclohexen-1-yl)-heptatrien-1,3,5-saeure-7-nitril

There total 17 articles about 3-Methyl-1-(2,6,6-trimethyl-cyclohexen-1-yl)-heptatrien-1,3,5-saeure-7-nitril which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: (4E,6E)-3-acetoxy-5-methyl-7-(2,6,6-trimethyl-1-cyclohexenyl)-4,6-heptadienenitrile

: 58526-71-9,59955-09-8
(2E,4E,6E)-5-methyl-7-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)-hepta-2,4,6-trienenal

Guidance literature:: With diazabicyclononane; In toluene; for 1.5h; Heating;

Reference yield: 37.0%

: 1209-68-3
3-methyl-5-(2,6,6-trimethylcyclohex-1-enyl)penta-2, 4-dienal

: 372-09-8
cyanoacetic acid

: 58526-71-9
3-Methyl-1-(2,6,6-trimethyl-cyclohexen-1-yl)-heptatrien-1,3,5-saeure-7-nitril

Guidance literature:: With piperidine; In benzene; at 0 ℃; for 18h; Reflux;

Reference yield:

: 2537-48-6
diethyl 1-cyanomethylphosphonate

: 3917-41-7
(2E,4E)-3-methyl-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2,4-pentadienal

: 58526-71-9,59955-09-8
(2E,4E,6E)-5-methyl-7-(2’,6’,6’-trimethylcyclohex-1’-en-1’-yl)-hepta-2,4,6-trienenal

Guidance literature:: diethyl 1-cyanomethylphosphonate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

(2E,4E)-3-methyl-5-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2,4-pentadienal; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 1h;
DOI:10.1021/ja4121814