Technology Process of C22H24F3N3O5
There total 5 articles about C22H24F3N3O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 4h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: ammonium formate / 5%-palladium/activated carbon / 7 h / 150 °C
2.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 6 h / Reflux
2.2: 0.5 h / 20 °C / pH 7 - 8
3.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C
With
thionyl chloride; ammonium formate; potassium carbonate;
5%-palladium/activated carbon; N,N-dimethyl-formamide;
In
dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetonitrile / 6 h / Reflux
2.1: nitric acid / acetic acid / 24 h / 20 °C / cooling with ice-water
3.1: ammonium formate / 5%-palladium/activated carbon / 7 h / 150 °C
4.1: thionyl chloride / N,N-dimethyl-formamide / dichloromethane / 6 h / Reflux
4.2: 0.5 h / 20 °C / pH 7 - 8
5.1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 80 °C
With
thionyl chloride; nitric acid; ammonium formate; potassium carbonate;
5%-palladium/activated carbon; N,N-dimethyl-formamide;
In
dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
