5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one

Base Information

Chemical Name:5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one
CAS No.:30390-18-2
Molecular Formula:C₂₅H₂₄O₅
Molecular Weight:404.463
Hs Code.:

Synonyms:5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one

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Chemical Property of 5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one

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Technology Process of 5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one

There total 6 articles about 5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 7058-70-0
5,7-dihydroxy-6-(2-methylbutanoyl)-8-(3-methylbut-2-enyl)-4-phenyl-2H-chromen-2-one

: 30390-18-2
5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one

Guidance literature:: With sodium hydrogencarbonate; palladium dichloride; In water; dimethyl sulfoxide; at 20 ℃; for 8h;
DOI:10.1016/j.phytochem.2004.07.001

Reference yield: 65.0%

: 31525-67-4
dimethylacetal of 3-methyl-3-hydroxybutyraldehyde

: 98192-58-6
5,7-Dihydroxy-6-(2-methylbutanoyl)-4-phenyl-2H-chromen-2-one

: 30390-18-2
5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one

Guidance literature:: In pyridine; at 160 ℃; for 48h;

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 30390-18-2
5-Hydroxy-8,8-dimethyl-6-(2-methylbutanoyl)-4-phenyl-2H,8H-benzo<1,2-b:3,4-b'>dipyran-2-one

Guidance literature:: Multi-step reaction with 3 steps

1: aluminium chloride / CS₂; nitromethane / Heating

2: 5percent sulfuric acid / acetic acid

3: pyridine / Heating

With aluminium trichloride; sulfuric acid; In pyridine; carbon disulfide; nitromethane; acetic acid;
DOI:10.1016/S0040-4039(00)98874-9