5-methoxy-3-benzyl-3H-benzindole

Base Information

Chemical Name:5-methoxy-3-benzyl-3H-benzindole
CAS No.:132205-82-4
Molecular Formula:C₂₀H₁₇NO
Molecular Weight:287.361
Hs Code.:

Synonyms:5-methoxy-3-benzyl-3H-benzindole

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Chemical Property of 5-methoxy-3-benzyl-3H-benzindole

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Technology Process of 5-methoxy-3-benzyl-3H-benzindole

There total 1 articles about 5-methoxy-3-benzyl-3H-benzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.8%

: 132205-81-3
trans-1-<2-(1-benzyl-1H-pyrrol-2-yl)-1-methoxyethenyl>benzene

: 132205-82-4
5-methoxy-3-benzyl-3H-benzindole

Guidance literature:: With triethylamine; 4-nitro-benzoic acid; palladium on activated charcoal; silica gel; In acetonitrile; 1.) 30 min, reflux, 2.) irradiation, 28 h;
DOI:10.1021/jo00006a052

Reference yield: 59.3%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 132205-82-4
5-methoxy-3-benzyl-3H-benzindole

: 124-40-3
dimethyl amine

: 132205-84-6
(3-Benzyl-5-methoxy-3H-benzo[e]indol-1-ylmethyl)-dimethyl-amine

: 132205-83-5
(3-Benzyl-5-methoxy-3H-benzo[e]indol-2-ylmethyl)-dimethyl-amine

Guidance literature:: With acetic acid; 1.) 0 deg C -> room temperature, 2.) 4 h;
DOI:10.1021/jo00006a052

Reference yield:

: 132205-82-4
5-methoxy-3-benzyl-3H-benzindole

: 132205-87-9
1-methyl-2-cyano-5-methoxy-3-benzylbenzindole

Guidance literature:: Multi-step reaction with 3 steps

1: 35.6 percent / glacial acetic acid / 1.) 0 deg C -> room temperature, 2.) 4 h

2: 89.7 percent / benzene

3: 27.1 percent / dimethylformamide / 4 h / Heating

With acetic acid; In N,N-dimethyl-formamide; benzene;
DOI:10.1021/jo00006a052