O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) stearyl glycyrrhetinate

Base Information

• Chemical Name: O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) stearyl glycyrrhetinate
• CAS No.: 1367192-03-7
• Molecular Formula: C₇₇H₁₁₂O₁₀
• Molecular Weight: 1197.73

Synonyms:O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) stearyl glycyrrhetinate

Chemical Property of O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) stearyl glycyrrhetinate

Chemical Property:

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Technology Process of O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) stearyl glycyrrhetinate

There total 1 articles about O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) stearyl glycyrrhetinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

C35H35O7PolS + glycyrrhetinyl stearate (13832-70-7) → O-(2-O-acetyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl) stearyl glycyrrhetinate (1367192-03-7)

Guidance literature:

C₃₅H₃₅O₇PolS; With 1-benzenesulfinyl piperidine; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.5h; Inert atmosphere; Molecular sieve; solid phase reaction;

With trifluoromethylsulfonic anhydride; In dichloromethane; at -60 ℃; for 0.0833333h; Inert atmosphere; Molecular sieve; solid phase reaction;

glycyrrhetinyl stearate; In dichloromethane; at -60 - 20 ℃; Inert atmosphere; Molecular sieve; solid phase reaction;

DOI:10.1039/c2ob06883d

upstream raw materials:

glycyrrhetinyl stearate

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