Technology Process of C23H15NO2S2
There total 3 articles about C23H15NO2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C16H11NOS2;
With
bis(2,2,6,6-tetramethylpiperidinyl)zinc, lithium chloride, magnesium chloride complex;
In
tetrahydrofuran;
at 25 ℃;
for 8h;
Inert atmosphere;
benzoyl chloride;
With
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran;
at 25 ℃;
for 2h;
Inert atmosphere;
DOI:10.1021/jo201250n
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: bis(2,2,6,6-tetramethylpiperidinyl)zinc, lithium chloride, magnesium chloride complex / tetrahydrofuran / 2 h / 25 °C / Inert atmosphere
1.2: 1 h / 25 °C / Inert atmosphere
2.1: bis(2,2,6,6-tetramethylpiperidinyl)zinc, lithium chloride, magnesium chloride complex / tetrahydrofuran / 8 h / 25 °C / Inert atmosphere
2.2: 2 h / 25 °C / Inert atmosphere
With
bis(2,2,6,6-tetramethylpiperidinyl)zinc, lithium chloride, magnesium chloride complex;
In
tetrahydrofuran;
DOI:10.1021/jo201250n
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: TurboGrignard / tetrahydrofuran / 0.5 h / -40 °C / Inert atmosphere
1.2: 0.5 h / -40 °C / Inert atmosphere
2.1: bis(2,2,6,6-tetramethylpiperidinyl)zinc, lithium chloride, magnesium chloride complex / tetrahydrofuran / 2 h / 25 °C / Inert atmosphere
2.2: 1 h / 25 °C / Inert atmosphere
3.1: bis(2,2,6,6-tetramethylpiperidinyl)zinc, lithium chloride, magnesium chloride complex / tetrahydrofuran / 8 h / 25 °C / Inert atmosphere
3.2: 2 h / 25 °C / Inert atmosphere
With
TurboGrignard; bis(2,2,6,6-tetramethylpiperidinyl)zinc, lithium chloride, magnesium chloride complex;
In
tetrahydrofuran;
DOI:10.1021/jo201250n
