(3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol

Base Information

Chemical Name:(3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol
CAS No.:828930-47-8
Molecular Formula:C₄₀H₅₈O₆
Molecular Weight:634.897
Hs Code.:

Synonyms:(3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol

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Chemical Property of (3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol

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Technology Process of (3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol

There total 3 articles about (3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 61490-28-6
1,3:4,6-di-O-benzylidene-D-mannitol

: 10340-84-8
(R)-8-bromo-2,6-dimethyloct-2-ene

: 828930-47-8
(3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 70 ℃; for 24h;
DOI:10.1016/j.bmc.2004.09.019

Reference yield:

: 69-65-8
mannitol

: 828930-47-8
(3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / sulfuric acid / dimethylformamide / 72 h / 20 °C

2: 52 percent / sodium hydride / dimethylformamide / 24 h / 70 °C

With sulfuric acid; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.09.019

Reference yield:

: 100-52-7
benzaldehyde

: 828930-47-8
(3'R)-1,3:4,6-di-O-benzylidene-2,5-di-O-(3',7'-dimethyl-6'-octenyl)-D-mannitol

Guidance literature:: Multi-step reaction with 2 steps

1: 26 percent / sulfuric acid / dimethylformamide / 72 h / 20 °C

2: 52 percent / sodium hydride / dimethylformamide / 24 h / 70 °C

With sulfuric acid; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2004.09.019