1-(3-hydroxyphenyl)prop-1-ene

Base Information

• Chemical Name: 1-(3-hydroxyphenyl)prop-1-ene
• CAS No.: 79755-53-6
• Molecular Formula: C₉H₁₀O
• Molecular Weight: 134.178
• Mol file: 79755-53-6.mol

Synonyms:1-(3-hydroxyphenyl)prop-1-ene

Chemical Property of 1-(3-hydroxyphenyl)prop-1-ene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-hydroxyphenyl)prop-1-ene

There total 13 articles about 1-(3-hydroxyphenyl)prop-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

ethyltriphenylphosphonium bromide (1530-32-1) + meta-hydroxybenzaldehyde (100-83-4) → 1-(3-hydroxyphenyl)prop-1-ene (79755-53-6)

Guidance literature:

ethyltriphenylphosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 2h; Inert atmosphere; Schlenk technique;

meta-hydroxybenzaldehyde; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 16h; Inert atmosphere; Schlenk technique;

DOI:10.1039/c8gc03823f

Reference yield: 79.0%

ethene (74-85-1) + 3-(non-8-enyl)phenol (1415155-47-3) → 1-(3-hydroxyphenyl)prop-1-ene (79755-53-6) + 3-hydroxystyrene (620-18-8,24979-69-9) + (E)-1-(3-hydroxyphenyl)-2-(3-hydroxyphenyl)ethene (70709-65-8,135781-00-9,143207-60-7)

Guidance literature:

ethene; 3-(non-8-enyl)phenol; With [1,3-bis(2,6-diisopropylphenyl)-2-imidazolidinylidene]dichloro[5-(isobutoxycarbonylamido)-2-isopropoxybenzylidene]ruthenium(II); di-μ-bromobis(tri-tertbutylphosphine)dipalladium(I); In cyclohexene; at 50 ℃; for 6h; under 750.075 Torr; Glovebox;

In cyclohexane; at 50 ℃; for 12h; Reagent/catalyst; Inert atmosphere;

DOI:10.1039/c7gc00553a

Reference yield: 77.0%

2-chloro-1-(3-hydroxyphenyl)propane (79755-52-5) → 1-(3-hydroxyphenyl)prop-1-ene (79755-53-6)

Guidance literature:

With potassium hydroxide; for 3h; Heating;

DOI:10.1039/P19810002570

upstream raw materials:

2-chloro-1-(3-hydroxyphenyl)propane

m-hydroxyphenylacetic acid

3-benzyloxyphenylacetic acid

<3-(benzyloxy)phenyl>acetone

Downstream raw materials:

3-n-propylphenol

(rac)-metaraminol