N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide

Base Information

Chemical Name:N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide
CAS No.:1071927-46-2
Molecular Formula:C₂₂H₁₈Cl₂F₆N₂O₂
Molecular Weight:527.294
Hs Code.:

Synonyms:N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide

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Chemical Property of N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide

Chemical Property:

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Technology Process of N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide

There total 5 articles about N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 407-62-5
5,5,5-trifluoropentanoic acid

: 1071927-10-0
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylaniline

: 1071927-46-2
N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield:

: 31680-07-6
4-methyl-3-nitrobenzaldehyde

: 1071927-46-2
N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide

Guidance literature:: Multi-step reaction with 5 steps

1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1 h / 20 °C

2: N-chloro-succinimide / N,N-dimethyl-formamide / 50 °C

3: triethylamine / N,N-dimethyl-formamide / 6 h / 20 °C

4: acetic acid / iron / ethanol; water / 1.25 h / 75 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; sodium acetate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; iron; In ethanol; water; N,N-dimethyl-formamide;

Reference yield:

: C₈H₇ClN₂O₃

: 1071927-46-2
N-(5-(5-(3,5-dichlorophenyl)-4,5-dihydro-5-trifluoromethyl-isoxazol-3-yl)-2-methyl-phenyl)-5,5,5-trifluoro-valeramide

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / N,N-dimethyl-formamide / 6 h / 20 °C

2: acetic acid / iron / ethanol; water / 1.25 h / 75 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 2 h / 20 °C

With acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; iron; In ethanol; water; N,N-dimethyl-formamide;