5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene

Base Information

Chemical Name:5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene
CAS No.:930110-41-1
Molecular Formula:C₁₇H₁₁Cl₂F₃N₂O₃
Molecular Weight:419.187
Hs Code.:

Synonyms:5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene

Chemical Property:

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Technology Process of 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene

There total 4 articles about 5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: C₈H₇ClN₂O₃

: 930110-41-1
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; Cooling with ice;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 5-hydroxyiminomethyl-2-methylnitrobenzene

: 930110-41-1
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene

Guidance literature:: 5-hydroxyiminomethyl-2-methylnitrobenzene; With N-chloro-succinimide; In N,N-dimethyl-formamide; at 50 ℃; for 1h;

1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene; With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

Reference yield:

: 31680-07-6
4-methyl-3-nitrobenzaldehyde

: 930110-41-1
5-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]-2-methylnitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1 h / 20 °C

2.1: N-chloro-succinimide / N,N-dimethyl-formamide / 1 h / 50 °C

2.2: 6 h / 20 °C

With N-chloro-succinimide; hydroxylamine hydrochloride; sodium acetate; In ethanol; water; N,N-dimethyl-formamide;